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肥猪散中制何首乌的薄层鉴别方法研究
单乃荣,余莲
0
(广西兽药监察所)
摘要:
建立了肥猪散中制何首乌的薄层色谱(TLC)定性鉴别法。以制何首乌为对照药材,采用甲苯-乙酸乙酯-甲酸(15:2:0.8)为展开剂,在UV365nm波长下检视,氨蒸气为显色剂,对肥猪散中制何首乌进行薄层色谱法鉴别。结果制何首乌斑点清晰,阴性无干扰。本方法简便,快速,结果准确,重现性好。可用于控制肥猪散的质量。
关键词:  肥猪散  制何首乌  TLC  质量控制
DOI:10.11751/ISSN.1002-1280.2017.5.08
投稿时间:2017-01-21修订日期:2017-04-29
基金项目:
Polygoni Multiflori Radlx Praeparata by TLC Identification in Feizhu Powder
单乃荣
(Guangxi Institute of Veterinary Drug Control)
Abstract:
To develop the Thin Layer Chromatography(TLC) identification for Polygoni Multiflori Radlx Praeparata in Feizhu San.Polygoni Multiflori Radlx Praeparata were identified by TLC,using physcion as chemical reference substances,methylbenzene-ethyl acetate-methanoic acid(15 :2:0.8)as mobile phases.The TLC chromatograms of Polygoni Multiflori Radlx Praeparata were of clearness,good separation,and no interference.The method is simple,quick,accurate,reproducible and can be used for the quality control of emodion of Feizhu San.
Key words:  Feizhu  Powder,Polygoni  Multiflori Radlx  Praeparata,TLC,Quality  contorl

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