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液相色谱-串联质谱法测定畜禽肉中十种磺胺类兽药残留的不确定度评定
任雪冬
0
(辽宁省分析科学研究院)
摘要:
本文依据GB/T20759-2006方法对畜禽肉中十种磺胺类兽药残留检测的不确定度进行了分析和评定。结果表明标准品的配制、稀释,标准曲线校准,样品回收率对样品的相对不确定度贡献较大。
关键词:  磺胺类兽药残留  液相色谱-串联质谱法  不确定度  评定
DOI:
投稿时间:2010-10-14修订日期:2011-03-08
基金项目:
Uncertainty Evaluation in the Determination of Ten Kinds of Sulfanilamide Residues in Poultry by Liquid Chromatography-Tandem Mass Spectrometry
renxuedong
(Liao Ning Province Academy of Analytic Science)
Abstract:
The article analyse and evaluate uncertainty in the determination of ten kings of sulfanilamides residues in poultry according to the method of GB/T20759-2006. The result makes known that contribution is major about the standard substance was confected and diluted、calibration of standard curve , coefficient of recovery of sample.
Key words:  sulfanilamides residues  Liquid Chromatography-Tandem Mass Spectrometry  uncertainty  evaluation

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